ANALYTICAL CHEMISTRY AND LABORATORY OF ANALYTICAL CHEMISTRY
Course unit partition: Cognomi M-Z

Academic year 2018/19
1° year of course - Second semester
Professor
Academic discipline
Chimica analitica (CHIM/01)
Field
Ambito aggregato per crediti di sede
Type of training activity
Caratterizzante
62 hours
of face-to-face activities
6 credits
hub: -
course unit
in ITALIAN

Learning objectives


The student gains the principles and the analytical procedures for the characterization of chemical compounds, possesses basic knowledge of quantitative chemical analysis, with reference to the analytical aspects of chemical equilibria, and to the methods of volumetric analysis. The student is also able to perform stoichiometric calculations and practical operations in relation to the preparation of solutions with known concentration and is able to choose and use the best method of separation, purification and analysis of chemical mixtures

Prerequisites


No

Course unit content

The course is focused on the systematic treatment of homogeneous and heterogeneous equilibria treated in an analytical key and applied to quantitative volumetric analyzes, proposed in the relative laboratory experiences

Full programme


Laboratory Demonstrations:
1. PRECIPITATION TITRATION AND ASSESSMENT OF THE ROBUSTNESS OF THE METHOD AS A FUNCTION OF THE AMOUNT OF INDICATOR

2. DETERMINATION OF THE TOTAL HARDNESS OF WATER WITH EDTA

3. DETERMINATION OF ALKALINITY AND 2 FREE CO2 IN WATER

4. DETERMINATION OF WATER OXIDABILITY ACCORDING TO KUBEL’S METHOD

5. DETERMINATION OF THE DISSOLVED OXYGEN ACCORDING TO WINKLER’S METHOD

6. DETERMINATION OF THE MAIN CONSTITUENTS OF "NORDISKT GULD" COINS (10, 20 AND 50 EUROCENT)

Bibliography


D. C. Harris; Chimica analitica quantitativa. Terza edizione italiana condotta sulla nona edizione americana; Ed. ZanichelliP. Michelin Lausarot – G. A. Vaglio; Stechiometria – Guida alla soluzione di problemi di Chimica: Ed. Piccin

Teaching methods


Frontal classes dealing with demonstrations concerning the systematic treatment of chemical equilibria, including the guided solution of problems relevant to the aforementioned equilibria. Description of the purposes, methods and procedures for the execution of the proposed laboratory practical demonstrations.

Assessment methods and criteria


The student compiles a laboratory report, in electronic format, showing the results and conclusions of the laboratory experience. After passing the written test, which requires the solution of problems and questions dealing with the chemical equilibria treated in the course, the student is admitted to the oral examination, during which the written test is discussed, the report and the overall knowledge of the arguments are verified.

Other information

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