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Università degli Studi di Parma Università degli Studi di Parma
Degree course in
Chemistry
Università degli Studi di Parma
Department of Chemistry, Life Sciences and Environmental Sustainability

LABORATORY FOR INORGANIC CHEMISTRY
cod. 07272

Academic year 2012/13
2° year of course - First semester
Professor
Academic discipline
Chimica generale e inorganica (CHIM/03)
Field
Attività formative affini o integrative
Type of training activity
Related/supplementary
69 hours
of face-to-face activities
6 credits
hub: -
course unit
in - - -
lectures timetable unavailable
exam calls

Integrated course unit module: INORGANIC CHEMISTRY AND LABORATORY

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Learning objectives

Principles of preparation of coordination compounds. Laboratory training. Spectroscopic techniques.

Prerequisites

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Course unit content

1) Synthesis of cis/trans-bis(glycinate)copper(II). Characterization by means of IR spectroscopy.
2) Synthesis of a NN donor ligand by a means of phase transfer catalysis. Synthesis of a Zn(II) complex. Characterization by means of NMR spectroscopy.
3) Synthesis of [Al(acetylacetonate)3] e [VO(acetylacetonate)2]. Characterization by means of NMR spectroscopy.
4) Preparation of d-tris(ethylenediamine) cobalt(III) triiodide by means of a partial asymmetric sysnthesis.
Description of the spectroscopic techniques (NMR, IR, UV-Vis).

Full programme

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Bibliography

1) Inorganic Chemistry (Shriver, Atkins)
2) Advanced Inorganic Chemistry
(Cotton)
3) Chemistry of the Elements
(Greenwood, Earnshaw)
4) Physical Methods in Advanced inorganic Chemistry (Hill, Day)
5) Infrared and Raman Spectra of Inorganic and Coordination Compounds (Nakamoto)
6) Spectrometric identification of organic compounds (Silverstein, Webster)

Teaching methods

Theoretical lessons and training in a synthetic laboratory.

Assessment methods and criteria

Written and oral examination.

Other information

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