FUNDAMENTALS OF CULTURAL HERITAGE-APPLIED SPECTROSCOPIC TECHNIQUES AND LAB
cod. 23683

Academic year 2010/11
3° year of course - First semester
Professor responsible for the course unit
LOTTICI Pier Paolo
integrated course unit
5 credits
hub:
course unit
in - - -

Learning objectives

The course aims to provide fundamental knowledge for understanding the most
important spectroscopic techniques used in diagnostic investigations of the cultural
heritage.

Students will acquire the essential notions to enable them to use laboratory
spectroscopy techniques, and will be able to identify pigments and/or minerals from
Raman or FT-IT measurements independently and from comparison with
spectroscopy databases.

Prerequisites

Attendance of courses in Experimental Physics and Introduction to Modern Physics

Course unit content

Spectroscopy and rudiments of quantum mechanics

Vibrational Spectroscopy Techniques

Full programme

Electromagnetic radiation and interactions with matter - Photons - Energy
transitions - Atomic spectroscopy - Absorption and emission - Vibrational
Spectroscopies - IR absorption - Raman - FTIR techniques - Micro-Raman -
Molecular spectroscopy - UV-VIS - XRF - X-ray fluorescence - X-ray absorption -
Thermoluminescence - LIBS (Light Induced Breakdown Spectroscopy) - notes on
XPS (X-ray Photoelectron Spectroscopy) - notes on NMR - Nuclear magnetic
resonance - notes on Mossbauer effect

Optics – Interferences and diffraction – Spectroscopy techniques and instruments –
Simple experiments in spectrum analysis – UV and VIS absorption – Vibrational
spectroscopy techniques: Raman and FT-IR, MicroRaman and FT-IR ATR – Case
studies – Minerals, pigments, colourants.

Bibliography

Notes and information provided by the professor

Teaching methods

Oral lesson
and experiments both in teaching and research laboratories
(Raman and FT-IR).

Assessment methods and criteria

Oral examination with discussion of the technique to case studies

Evaluation of a written report on a proposed experiment and follow-up identifying
types of pigments in artefacts by means of vibrational spectroscopy

Other information

- - -