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Università degli Studi di Parma Università degli Studi di Parma
University of Parma
Course catalogue
Università degli Studi di Parma
course catalogue

LABORATORY FOR INSTRUMENTAL ANALYTICAL CHEMISTRY
cod. 06670

Academic year 2008/09
2° year of course - First semester
Professor
Academic discipline
Chimica analitica (CHIM/01)
Field
Discipline analitiche e ambientali
Type of training activity
Characterising
60 hours
of face-to-face activities
4 credits
hub: -
course unit
in - - -
lectures timetable unavailable
exam calls
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Learning objectives

<br />Practical application of instrumental analytical chemistry thecniques (HPLC, GC, ICP, UV, IR, XRD) and to provide the basic concept of the statistical data treatment.

Prerequisites

General and Inorganic Chemistry. Analytical Chemistry.

Course unit content

<br />Development of an analytical method.<br />Qualitative and quantitative analysis.<br />Excercises on the calculation of solution concentration and dilution.<br />Introduction to validation criteria: definition of the quality parameter of ana analytical method.<br />Calibration thecniques: <br />external standard method<br />Internal standard method<br />Statistical tests for the evaluation of linearity. <br />Laboratory experiments:<br />Theoretical aspects of the laboratory experiments.<br />Colorimetric UV-vis determination of Fe2+ in water<br />Spectrophotometric atomic emission determination of metals.<br />Anion exchange HPLC with conduttimetric detection for the determination of anions in water.<br />HPLC-UV determination of alkylphenols in water.<br />FT-IR analysis of a liquid and a solid substance<br />Powder analysis by XR diffraction.<br />Determination of volatile compounds by gaschromatography with different detection thecniques and use of internal standard.<br />Statistical data treatment with Excel.<br />

Full programme

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Bibliography

<br />D.A. Skoog, D.M. West, F.J. Holler, Fondamenti di Chimica Analitica EdiSES, Napoli; <br />D.C. Harris, Chimica Analitica Quantitativa, Zanichelli, Bologna

Teaching methods

<br />Oral lectures and Laboratory.<br />Oral exam

Assessment methods and criteria

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Other information

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